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Nitration. Nitration of aromatic hydrocarbons is a well-studied area covered in monographs and review papers. 47- 56 Nitration may be accomplished by a number of reagents, most commonly by a mixture of nitric acid and sulfuric acid (mixed acid). Additional important reagents are dinitrogen tetroxide in the presence of acidic catalysts, dinitrogen pentoxide under anhydrous conditions, 57 alkyl and acyl nitrates, and nitronium salts. Metallic nitrates impregnated on KlO montmorillonite were shown to nitrate alkylbenzenes to yieldp-nitroalkylbenzenes with high selectivity 4,35,58 The highest para selectivity was, however, achieved by 9-nitroanthracene. The 9-nitroanthracenium ion formed under superacidic catalysis (NafionH) effects transfer nitration of toluene to give p-nitrotoluene with >95% selectivity albeit in low yields 5%).59 As the use of mixed acid results in spent (diluted) acid, causing serious environmental disposal problems in industrial applications, solid acid catalysts, such as cl ays 34,35 or high-acidity resins (Nafion-H,60-63 etc.), are gaining importance. Our basic knowledge of electrophilic nitration of aromatic hydrocarbons results from the work of Ingold,24 who established that the nitronium cation is the true reactive electrophile in these reactions. 64-67 In the traditional nitration process with the mixed acid the nitronium cation is generated according to Eqs. (l0.4) and (l0.5): barcode excel 2010 gratis How to generate a barcode in Excel | Sage Intelligence
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